تهیه جاذب فیلمی نوین بر پایه کربن فعال مغناطیسی/آلژینات و ارزیابی کارایی آن در حذف رنگزای کریستال ویولت از آب

نوع مقاله : مقاله پژوهشی

نویسندگان

دانشکده مهندسی شیمی و نفت، دانشگاه تبریز، تبریز، ایران، صندوق‌پستی: 51666-16471

چکیده

این مطالعه با هدف سنتز یک جاذب جدید و ارزان‌قیمت به شکل فیلم از منبع طبیعی و در دسترس هسته سنجد، با روش تهیه آسان، و همچنین بازدهی بالاتر از 90 درصد در جذب رنگزای کریستال ویولت انجام شده است. با بررسی تأثیر عوامل مختلف از قبیل pH، مقدار جاذب، دما، زمان تماس و غلظت اولیه رنگزا، شرایط بهینه بیشینه جذب مشخص گردید. نتایج نشان دادند بیشینه بازده جذب 94.24 درصد بوده و در شرایط بهینه شامل 8 = pH، مقدار جاذب g/l1، دمای ºC 25، زمان تماس min 90 و غلظت اولیه رنگزا mg/l 10 به دست می­آید. با بررسی مدل­های ایزوترمی و سینتیکی مشخص شد که جذب به صورت فیزیکی و مطلوب بوده و داده­های تعادلی با مدل ایزوترم لانگمویر و مدل سینتیکی شبه مرتبه دوم برازش بیشتری دارند. بیشینه ظرفیت جذب جاذب فیلمی
mg/g 30.30 محاسبه شد. بررسی ترمودینامیکی نشان داد که جذب به صورت خودبه‌خودی و گرمازا اتفاق می­افتد. مطالعات واجذبی نیز بیان کرد که بعد از چندین مرحله دفع متوالی، همچنان ظرفیت جذب جاذب مطلوب است.

کلیدواژه‌ها

عنوان مقاله [English]

Preparation of a New Adsorbent Film Based on Magnetic Activated Carbon/ Alginate and Evaluation of its Efficiency in Crystal Violet Removal from Water

نویسندگان [English]

  • M. Chaharkam
  • M. Tahmasebpoor
Faculty of Chemical & Petroleum Engineering, University of Tabriz, P.O. Box: 51666-16471, Tabriz, Iran.
چکیده [English]

This study aims to synthesize a novel low-cost adsorbent in the form of film prepared by natural and available sources of elderberry kernel, with an easy preparation method and an efficiency higher than 90% in the adsorption of crystal violet dye. By investigating the effects of various parameters, including pH, adsorbent dose, temperature, contact time and dye initial concentration, the optimum conditions to reach the maximum adsorption were determined. Results showed that the maximum adsorption efficiency is 94.24 %, which is obtained under optimal conditions of
pH = 8, adsorbent dose 1 g/l, temperature 25 °C, contact time 90 min and dye initial concentration 10 mg/l. Isotherm and kinetic models reveal that the adsorption is physical and favourable, and equilibrium data are more compatible with Langmuir isotherm and pseudo-second-order kinetic models. The maximum adsorption capacity of adsorbent was calculated to be 30.30 mg/g. Thermodynamic investigation showed that the adsorption is spontaneous and exothermically. Desorption studies also stated that after several consecutive removal steps, the adsorption capacity is still favourable.

کلیدواژه‌ها [English]

  • Adsorbent film
  • Activated carbon
  • Alginate
  • Adsorption
  • Crystal violet

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